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E4F - C Graphitic

A 0.5 g sample is subjected to a multistage furnace treatment to remove all forms of carbon with the exception of graphitic carbon. Either a resistance or induction furnace is used for analysis.  The inductive elements of the sample and accelerator couple with the high frequency field of the induction furnace. The pure oxygen environment and the heat generated by this coupling cause the sample to combust. During combustion, carbon-bearing elements are reduced, releasing the carbon, which immediately binds with the oxygen to form CO and CO2, the majority being CO2. Carbon is measured as carbon dioxide in the IR cell as gases flow through the IR cells.  Carbon dioxide absorbs IR energy at a precise wavelength within the IR spectrum.  Energy from the IR source is absorbed as the gas passes through the cell, preventing it from reaching the IR detector.  All other IR energy is prevented from reaching the IR detector by a narrow bandpass filter.  Because of the filter, the absorption of IR energy can be attributed only to carbon dioxide (CO2). The concentration of COis detected as a reduction in the level of energy at the detector.

 

Analysis

Method

Reporting Limit

E4F-C Graphitic

IR

0.05%




Activation Laboratories Ltd. | 41 Bittern Street, Ancaster, Ontario, L9G 4V5, Canada | TF: +1.888.228.5227
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