Weblims     OWA     Home     Contact Us    

Actlabs
Back to Home


7 of 146    Prev    Next     

1A2 - (1A2-30 or 50) Au Fire Assay - AA

Fire Assay Fusion

A sample size of 5 to 50 grams can be used but the routine size is 30 g for rock pulps, soils or sediments (exploration samples). The sample is mixed with fire assay fluxes (borax, soda ash, silica, litharge) and with Ag added as a collector and the mixture is placed in a fire clay crucible. The mixture is then preheated at 850°C, intermediate 950°C and finish 1060°C with the entire fusion process lasting 60 minutes. The crucibles are then removed from the assay furnace and the molten slag (lighter material) is carefully poured from the crucible into a mould, leaving a lead button at the base of the mould. The lead button is then placed in a preheated cupel which absorbs the lead when cupelled at 950°C to recover the Ag (doré bead) + Au.

 

AA Finish

The entire Ag dore bead is dissolved in aqua regia and the gold content is determined by AA (Atomic Absorption). AA is an instrumental method of determining element concentration by introducing an element in its atomic form, to a light beam of appropriate wavelength causing the atom to absorb light. The reduction in the intensity of the light beam directly correlates with the concentration of the elemental atomic species.On each tray of 42 samples there is two blanks, three sample duplicates and 2 certified reference materials, one high and one low (QC 7 out of 42 samples). We generally rerun all gold by fire assay gravimetric over 5,000 ppb to ensure accurate values

 

 

Code 1A2   (Fire Assay-AA) Detection Limits (ppb)

Element

Detection

Limit

Upper

Limit

Au

5

5,000

 

Note: If value exceeds upper limit, reanalysis by Fire Assay-Gravimetric (Code 1A3) is recommended.

 

Reference:

Hoffman, E.L., Clark, J.R. and Yeager, J.R. 1998. Gold analysis - Fire Assaying and alternative methods. Exploration and Mining Geology, Volume 7, pp. 155-160.

 


Activation Laboratories Ltd. | 41 Bittern Street, Ancaster, Ontario, L9G 4V5, Canada | TF: +1.888.228.5227
Search | Privacy | Contact Us | News RSS | Login