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Ultratrace 7 - Peroxide Fusion - ICP and ICP/MS

Ultratrace 7 combines a Sodium Peroxide Fusion with ICP and ICP/MS. All metals are solubilized.


ICP/MS

Fused samples are diluted and analyzed by Perkin Elmer Sciex ELAN 6000, 6100 or 9000 ICP/MS. Fused blank is run in triplicate for every 22 samples. Controls and standards fused with samples are run after the 22 samples. Fused duplicates are run every 10 samples. Instrument is recalibrated every 44 samples.

 

ICP/OES

Samples are analyzed with a minimum of 10 certified reference materials for the required analytes, all prepared by sodium peroxide fusion. Every 10th sample is prepared and analyzed in duplicate; a blank is prepared every 30 samples and analyzed. Samples are analyzed using a Varian 735ES ICP and internal standards are used as part of the standard operating procedure.  

 

Code Ultratrace-7 Elements and Detection Limits (ppm)

Element

Detection Limit

Upper Limit

Reported By

Element

Detection Limit

Upper Limit

Reported By

Al

0.01%

25%

ICP

Mo

1

10,000

ICP/MS

As

5

10,000

ICP/MS

Nb

2.4

5,000

ICP/MS

B

10

10,000

ICP/MS

Nd

0.4

5,000

ICP/MS

Ba

3

10,000

ICP/MS

Ni

10

10,000

ICP/MS

Be

3

5,000

ICP/MS

Pb

0.8

5,000

ICP/MS

Bi

2

5,000

ICP/MS

Pr

0.1

1,000

ICP/MS

Ca

0.01%

40%

ICP

Rb

0.4

5,000

ICP/MS

Cd

2

5,000

ICP/MS

S

0.01%

25%

ICP

Ce

0.8

5,000

ICP/MS

Sb

2

5,000

ICP/MS

Co

0.2

5,000

ICP/MS

Se

0.8

5,000

ICP/MS

Cr

30

10,000

ICP/MS

Si

0.01%

30%

ICP

Cs

0.1

5,000

ICP/MS

Sm

0.1

1,000

ICP/MS

Cu

2

10,000

ICP/MS

Sn

0.5

10,000

ICP/MS

Dy

0.3

5,000

ICP/MS

Sr

3

10,000

ICP/MS

Er

0.1

5,000

ICP/MS

Ta

0.2

10,000

ICP/MS

Eu

0.1

1,000

ICP/MS

Tb

0.1

1,000

ICP/MS

Fe

0.05%

30%

ICP

Te

6

10,000

ICP/MS

Ga

0.2

5,000

ICP/MS

Th

0.1

1,000

ICP/MS

Ge

0.7

5,000

ICP/MS

Ti

0.01%

25%

ICP

Gd

0.1

5,000

ICP/MS

Tl

0.1

1,000

ICP/MS

Hf

10

5,000

ICP/MS

Tm

0.1

1,000

ICP/MS

Ho

0.2

1,000

ICP/MS

U

0.1

10,000

ICP/MS

In

0.2

1,000

ICP/MS

V

5

10,000

ICP/MS

K

0.1%

25%

ICP

W

0.7

5,000

ICP/MS

La

0.4

10,000

ICP/MS

Y

0.1

1,000

ICP/MS

Li

3

10,000

ICP/MS

Yb

0.1

1,000

ICP/MS

Mg

0.01%

30%

ICP

Zn

25

10,000

ICP/MS

Mn

3

10,000

ICP/MS





 

 

 

 


Activation Laboratories Ltd. | 41 Bittern Street, Ancaster, Ontario, L9G 4V5, Canada | TF: +1.888.228.5227
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